[0082] (1) Dissolve 150mL of ethanol solution with 2-(2-aminoethoxy)ethanol 2 as the starting material (100mmol, 10.5g), and add di-tert-butyl dicarbonate (100mmol, 23mL) dropwise under ice bath conditions , removed the ice bath, reacted at room temperature for 2h, distilled off the ethanol solvent under reduced pressure
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